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Beilstein J. Org. Chem. 2014, 10, 141–149, doi:10.3762/bjoc.10.11
Graphical Abstract
Scheme 1: Reaction of active methylenenitriles with α,β-unsaturated ketones 1.
Scheme 2: Synthesis of 2-amino-4-phenyl-3-cyanopyridines 2.
Scheme 3: Synthesis of polysubstituted benzenes 3.
Scheme 4: Syntheses of compound 9 and compounds 13a,b.
Figure 1: X-ray crystal structure of 9.
Figure 2: X-ray crystal structure of 13a.
Figure 3: X-ray crystal structure of 18.
Scheme 5: Syntheses of compounds 18 and 21.
Figure 4: X-ray crystal structure of 21.
Figure 5: X-ray crystal structure of 26.
Scheme 6: Syntheses of compound 26.
Figure 6: X-ray crystal structure of 27a.
Scheme 7: Syntheses of compound 28a,b.
Figure 7: X-ray crystal structure of 28b.
Figure 8: X-ray crystal structure of 31a.
Figure 9: X-ray crystal structure of 31b.
Scheme 8: Syntheses of compound 31a,b.
Scheme 9: Syntheses of compound 33a,b.
Figure 10: X-ray crystal structure of 33a.
Scheme 10: Syntheses of compound 37a–c.
Figure 11: X-ray crystal structure of 37a.
Figure 12: X-ray crystal structure of 37b.
Scheme 11: Syntheses of compounds 38–40.
Figure 13: X-ray crystal structure of 39.